JPH0621165Y2 - 電子顕微鏡用試料凍結乾燥装置 - Google Patents
電子顕微鏡用試料凍結乾燥装置Info
- Publication number
- JPH0621165Y2 JPH0621165Y2 JP7811688U JP7811688U JPH0621165Y2 JP H0621165 Y2 JPH0621165 Y2 JP H0621165Y2 JP 7811688 U JP7811688 U JP 7811688U JP 7811688 U JP7811688 U JP 7811688U JP H0621165 Y2 JPH0621165 Y2 JP H0621165Y2
- Authority
- JP
- Japan
- Prior art keywords
- sample
- chamber
- electron microscope
- drying
- freeze
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000004108 freeze drying Methods 0.000 title claims description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000003960 organic solvent Substances 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 8
- 238000007710 freezing Methods 0.000 claims description 7
- 230000008014 freezing Effects 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000000523 sample Substances 0.000 description 45
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 24
- 238000000034 method Methods 0.000 description 13
- 238000001035 drying Methods 0.000 description 12
- 239000012472 biological sample Substances 0.000 description 8
- 239000007788 liquid Substances 0.000 description 4
- 238000000352 supercritical drying Methods 0.000 description 4
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 239000003595 mist Substances 0.000 description 3
- 230000000717 retained effect Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 239000012520 frozen sample Substances 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000000859 sublimation Methods 0.000 description 2
- 230000008022 sublimation Effects 0.000 description 2
- AJDIZQLSFPQPEY-UHFFFAOYSA-N 1,1,2-Trichlorotrifluoroethane Chemical compound FC(F)(Cl)C(F)(Cl)Cl AJDIZQLSFPQPEY-UHFFFAOYSA-N 0.000 description 1
- 241000048246 Gallicrex cinerea Species 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 230000000877 morphologic effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000001073 sample cooling Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 238000012876 topography Methods 0.000 description 1
Landscapes
- Sampling And Sample Adjustment (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7811688U JPH0621165Y2 (ja) | 1988-06-13 | 1988-06-13 | 電子顕微鏡用試料凍結乾燥装置 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP7811688U JPH0621165Y2 (ja) | 1988-06-13 | 1988-06-13 | 電子顕微鏡用試料凍結乾燥装置 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02147U JPH02147U (en]) | 1990-01-05 |
| JPH0621165Y2 true JPH0621165Y2 (ja) | 1994-06-01 |
Family
ID=31303065
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP7811688U Expired - Lifetime JPH0621165Y2 (ja) | 1988-06-13 | 1988-06-13 | 電子顕微鏡用試料凍結乾燥装置 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0621165Y2 (en]) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3053731B2 (ja) * | 1994-04-13 | 2000-06-19 | 日本電子株式会社 | 走査電子顕微鏡用生物試料作製方法および生物試料観察方法 |
| EP2755225B1 (en) * | 2011-09-09 | 2017-05-10 | Japan Science and Technology Agency | Electron-microscopic examination method for examining a living biological sample |
| JP2021135141A (ja) * | 2020-02-26 | 2021-09-13 | 国立研究開発法人産業技術総合研究所 | 粒子評価用標本の作製装置及び作製方法 |
-
1988
- 1988-06-13 JP JP7811688U patent/JPH0621165Y2/ja not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| JPH02147U (en]) | 1990-01-05 |
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